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Dispersed Nickel Oxide Films for Electro-oxidation of 1, 4-Butanediol

• J.Chem.Soc.Pak., Vol. 33, No. 1, 2011
 The potentiodynamic response of the

nickel/alkaline aqueous solution inter-face in the

region of the hydrated Ni(OH)2 to NiOOH

electrochemical reaction revealed that both species

undergo phase transformations [1]. The anodic

product from the Ni(OH)2 species involves the

formation of three species energetically different

which are detected during the electro-reduction

process. Under well-defined perturbation conditions,

a reasonable set of kinetic parameters pertaining to

the anodic process was obtained which was formally

interpreted through a consecutive three-step

mechanism of reaction involving a charge transfer, a

chemical reaction, and a charge transfer and a proton

transfer process. Side reactions involved water take

in account to various aging processes of the reaction


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